Effect of Hydrofluoric Acid Etching Time on Flexural Strength and Surface Roughness of CAD/CAM Ceramic Materials
DOI:
https://doi.org/10.35516/jmj.v59i1.2602Keywords:
Flexural, Strength, Surface Roughness, Ceramic Materials, Dental RestorationsAbstract
Objective: This study emulated the influences of varied hydrofluoric acid etching durations on the flexural strength and surface roughness of three CAD/CAM dental glass ceramic materials: feldspathic—CEREC blocs CPC, leucite-reinforced—IPS Empress CAD, and lithium disilicate—IPS e.max CAD.
Methods: The samples were prepared and divided with respect to the type of material to be etched for 0, 20, 60, and 90 seconds. This was followed by ultrasonic cleaning and successive thermocycling. SR and FS were measured with the profilometer and by the 3-point bending test, respectively. Data were statistically analyzed using ANOVA.
Results: The results indicated that increasing HF etching time significantly reduced the FS of the lithium disilicate group only, thus being dependent on material composition, p < 0.05. In all materials, SR increased with longer etching time. This increase in SR with deeper etching therefore places a direct relationship between etching time and surface texture.
Conclusion: This paper points out that one of the most critical factors in regard to the optimization of mechanical properties in ceramic materials for dental restorations is HF etching time. The choice of appropriate etching times relative to what exists is essential for the ultimate clinical performance and lifetime of ceramic restorations, with chosen durations favoring specific materials over others. This information is very valuable for dental practitioners in making appropriate choices toward durability and reliability in ceramic dental restorations.
References
Saadallah S, Al-Azzawi AKJ. The Influence of Different Fabrication and Impression Techniques on the Marginal Adaptation of Lithium Disilicate Crowns (A comparative in vitro study). Journal of Baghdad College of Dentistry. 2017;29(4):20-6.
Kang SH, Chang J, Son HH. Flexural strength and microstructure of two lithium disilicate glass ceramics for CAD/CAM restoration in the dental clinic. Restorative dentistry & endodontics. 2013;38(3):134-40.
Abdulla HA, Majeed MAJIJoFM, Toxicology. Assessment of bioactive resin-modified glass ionomer restorative as a new CAD/CAM material. Part I: Marginal fitness study. 2020;14(1):865.
Al-Joboury AI, Zakaria MR, J MM. An evaluation of the influence of different finishing lines on the fracture strength of full contour zirconia CAD/CAM and heat press all-ceramic crowns. Journal of Baghdad College of Dentistry. 2015;27(1):54-62.
Puppin-Rontani J, Sundfeld D, Costa AR, Correr AB, Puppin-Rontani RM, Borges GA, et al. Effect of Hydrofluoric Acid Concentration and Etching Time on Bond Strength to Lithium Disilicate Glass Ceramic. Operative dentistry. 2017;42(6):606-15.
Ozcan M, Allahbeickaraghi A, Dündar M. Possible hazardous effects of hydrofluoric acid and recommendations for treatment approach: a review. Clinical oral investigations. 2012;16(1):15-23.
Venturini AB, Prochnow C, May LG, Bottino MC, Felipe Valandro L. Influence of hydrofluoric acid concentration on the flexural strength of a feldspathic ceramic. Journal of the mechanical behavior of biomedical materials. 2015;48:241-8.
Prochnow C, Venturini AB, Grasel R, Bottino MC, Valandro LF. Effect of etching with distinct hydrofluoric acid concentrations on the flexural strength of a lithium disilicate-based glass ceramic. Journal of biomedical materials research Part B, Applied biomaterials. 2017;105(4):885-91.
Veríssimo AH, Moura DMD, Tribst JPM, Araújo AMM, Leite FPP, Souza R. Effect of hydrofluoric acid concentration and etching time on resin-bond strength to different glass ceramics. Brazilian oral research. 2019;33:e041.
Shakir G, Hameed M. Influence of Simulated Gastric Juice on Surface Roughness, Morphology and Micro Hardness of CAD-CAM Materials (An In Vitro Study). Journal of Research in Medical and Dental Science. 2022;10:058-65.
Jassim SJ, Majeed MA. Effect of plasma surface treatment of three different CAD/CAM materials on the micro shear bond strength with resin cement (A comparative in vitro study). Heliyon. 2023;9(7):e17790.
Prochnow C, Venturini AB, Grasel R, Bottino MC ,
Valandro LFJJoBMRPBAB. Effect of etching with distinct hydrofluoric acid concentrations on the flexural strength of a lithium disilicate‐based glass ceramic. 2017;105(4):885-91.
Abdulla HA, Majeed MAJJRMDS. Assessment of Bioactive Resin-modified Glass Ionomer Restorative as a New CAD/CAM Material Part II: Fracture Strength Study. 2019;7:74-9.
Altamimi A, Abdulrahman M. Development and Assessment of a New Bioactive Glass Fiber Post Part I: Flexural Strength and Fatigue Resistance. Journal of Research in Medical and Dental Science. 2021;9:16-24.
Venturini AB, Prochnow C, May LG, Bottino MC, Valandro LFJJotMBoBM. Influence of hydrofluoric acid concentration on the flexural strength of a feldspathic ceramic. 2015;48:241-8.
Cengiz-Yanardag E ,Kurtulmus Yilmaz S, Karakaya I, Ongun SJJoAS, Technology. Effect of Different Surface Treatment Methods on Micro-Shear Bond Strength of CAD-CAM Restorative Materials to Resin Cement. 2019;33(2):110-23.
Tokar E, Polat S, Ozturk C. Repair bond strength
of composite to Er,Cr:YSGG laser irradiated zirconia and porcelain surfaces. Biomedical journal. 2019;42(3):193-9.
Sinaga VR, Bonifacius S, Sumarsongko TJPJoD. Shear bond strength of two ceramic repair system to lithium disilicate: An in-vitro comparison. 2021;33(2):139-45.
Pedrazzi H, Takeuchi CY, Cioffi SS, Galvão MR, De Andrade MF, Bezzon OL. Shear bond strength of repairs in porcelain conditioned with laser. Microscopy research and technique. 2012;75(12):1639-45.
Kilinc H, Sanal FA, Turgut S. Shear bond strengths of aged and non-aged CAD/CAM materials after different surface treatments. The journal of advanced prosthodontics. 2020;12(5):273-82.
An HS, Park JM, Park EJ. Evaluation of shear bond strengths of gingiva-colored composite resin to porcelain, metal and zirconia substrates. The journal of advanced prosthodontics. 2011;3(3):166-71.
Morresi AL, D'Amario M, Capogreco M, Gatto R, Marzo G, D'Arcangelo C, et al. Thermal cycling for restorative materials: does a standardized protocol exist in laboratory testing? A literature review. Journal of the mechanical behavior of biomedical materials. 2014;29:295-308.
Falah RM, Ameer ZMAJJoRiM, Science D. Shear Bond Strength of Aged CAD/CAM Ceramic Materials Repaired by Resin Composite In vitro Using Different Repair Adhesives. 2020;8(1):61-7.
Zogheib LV, Bona AD, Kimpara ET, McCabe JF. Effect of hydrofluoric acid etching duration on the roughness and flexural strength of a lithium disilicate-based glass ceramic. Brazilian dental journal. 2011;22(1):45-50.
Bona AD, Anusavice KJ, Hood JAJIJoP. Effect of ceramic surface treatment on tensile bond strength to a resin cement. 2002;15 ( 3 .)
Addison O, Marquis PM, Fleming GJ. The impact of hydrofluoric acid surface treatments on the
performance of a porcelain laminate restorative material. Dental materials : official publication of the Academy of Dental Materials. 2007;23(4):461-
Kukiattrakoon B, Thammasitboon K. The effect of different etching times of acidulated phosphate fluoride gel on the shear bond strength of high-leucite ceramics bonded to composite resin. The Journal of prosthetic dentistry. 2007;98(1):17-23.
Barghi N, Fischer DE, Vatani L. Effects of porcelain leucite content, types of etchants, and etching time on porcelain-composite bond. Journal of esthetic and restorative dentistry : official publication of the American Academy of Esthetic Dentistry [et al]. 2006;18(1):47-52; discussion 3.
Magne P, Cascione D. Influence of post-etching cleaning and connecting porcelain on the microtensile bond strength of composite resin to feldspathic porcelain. The Journal of prosthetic dentistry. 2006;96(5):354-61.
Mecholsky JJ, Jr. Fractography: determining the sites of fracture initiation. Dental materials : official publication of the Academy of Dental Materials. 1995;11(2):113-6.
Naves LZ, Soares CJ, Moraes RR, Gonçalves LS, Sinhoreti MA, Correr-Sobrinho L. Surface/interface morphology and bond strength to glass ceramic etched for different periods. Operative dentistry. 2010; 35(4): 420-7.
Straface A, Rupp L, Gintaute A, Fischer J, Zitzmann NU, Rohr N. HF etching of CAD/CAM materials: influence of HF concentration and etching time on shear bond strength. Head & face medicine. 2019;15(1):21.
Sundfeld Neto D, Naves LZ, Costa AR, Correr AB, Consani S, Borges GA, et al. The Effect of Hydrofluoric Acid Concentration on the Bond Strength and Morphology of the Surface and Interface of Glass Ceramics to a Resin Cement. Operative dentistry. 2015;40(5):470-9.
Kansu G, Gökdeniz BJJoDS. Effects of different surface-treatment methods on the bond strengths of resin cements to full-ceramic systems. 2011;6(3):134-9.